Chemical transformation and morphology change of nickel–silica hybrid nanostructures via nickel phyllosilicates

Ji Chan Park; Hyun Ju Lee; Jung Up Bang; Kang Hyun Park; Hyunjoon Song

doi:10.1039/B916837K

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Chemical Communications

Issue 47, 2009

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Chemical transformation and morphology change of nickel–silica hybrid nanostructures via nickel phyllosilicates

Ji Chan Park , Hyun Ju Lee , Jung Up Bang , Kang Hyun Park and Hyunjoon Song

Chem. Commun., 2009, 7345-7347

DOI: 10.1039/B916837K
Received 14 Aug 2009, Accepted 14 Oct 2009
First published on the web 26 Oct 2009

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Abstract
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Ni@SiO₂ core-shell nanoparticles were transformed to Ni particles on silica spheres via a branched nickel phyllosilicate phase by hydrothermal and hydrogen reduction reactions; the final morphology was successfully employed as an active nanocatalyst for the hydrogen transfer reaction of acetophenone.

Supplementary Info

Details of experimental procedures, XRD spectra, N₂ sorption isotherms, and TEM and HRTEM images of theproducts, and ¹H-NMR spectra of the reactants and products in hydrogentransfer reactions
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Ji Chan Park
Hyun Ju Lee
Jung Up Bang
Kang Hyun Park
Hyunjoon Song

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Chemical Communications

Chemical transformation and morphology change of nickel–silica hybrid nanostructures via nickel phyllosilicates

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