Encapsulated chloride coordinating with two in–in protons of bridgehead amines in an octaprotonated azacryptand

Musabbir A. Saeed; Frank R. Fronczek; Md. Alamgir Hossain

doi:10.1039/B916099J

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Chemical Communications

Issue 42, 2009

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Encapsulated chloride coordinating with two in–in protons of bridgehead amines in an octaprotonated azacryptand

Musabbir A. Saeed , Frank R. Fronczek and Md. Alamgir Hossain

Chem. Commun., 2009, 6409-6411

DOI: 10.1039/B916099J
Received 05 Aug 2009, Accepted 11 Sep 2009
First published on the web 02 Oct 2009

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Abstract
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An encapsulated chloride in a thiophene-based cryptand is bridged by two in–in protons of tertiary amines with an NCl⁻ distance of 3.048(3) Å, similar to that observed in Park and Simmons’ katapinand chloride complex.

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Chemical Communications

Encapsulated chloride coordinating with two in–in protons of bridgehead amines in an octaprotonated azacryptand

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