Synthesis of fluorinated allenes via palladium-catalyzed monofluoromethylation using FBSM

Masamichi Ogasawara; Hidetoshi Murakami; Tatsuya Furukawa; Tamotsu Takahashi; Norio Shibata

doi:10.1039/B912531K

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Chemical Communications

Issue 47, 2009

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Synthesis of fluorinated allenes via palladium-catalyzed monofluoromethylation using FBSM

Masamichi Ogasawara , Hidetoshi Murakami , Tatsuya Furukawa , Tamotsu Takahashi and Norio Shibata

Chem. Commun., 2009, 7366-7368

DOI: 10.1039/B912531K
Received 25 Jun 2009, Accepted 16 Oct 2009
First published on the web 02 Nov 2009

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Palladium-catalyzed monofluoromethylation of substituted 2-bromo-1,3-dienes using fluorobis(phenylsulfonyl)methane (FBSM) as a pronucleophile gave previously unknown monofluoromethylated allenes in high yields, which are the isosteres of biologically attractive allenic alcohols.

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Masamichi Ogasawara
Hidetoshi Murakami
Tatsuya Furukawa
Tamotsu Takahashi
Norio Shibata

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Chemical Communications

Synthesis of fluorinated allenes via palladium-catalyzed monofluoromethylation using FBSM

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