Total synthesis of (+)-virgatusin via AlCl3-catalyzed [3+2] cycloaddition

Shanina D. Sanders; Andrea Ruiz-Olalla; Jeffrey S. Johnson

doi:10.1039/B911765B

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Chemical Communications

Issue 34, 2009

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Total synthesis of (+)-virgatusin via AlCl₃-catalyzed [3+2] cycloaddition

Shanina D. Sanders , Andrea Ruiz-Olalla and Jeffrey S. Johnson

Chem. Commun., 2009, 5135-5137

DOI: 10.1039/B911765B
Received 16 Jun 2009, Accepted 13 Jul 2009
First published on the web 27 Jul 2009
This article is part of the collection: Selective Catalysis for Organic Synthesis

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Abstract
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The AlCl₃-catalyzed cycloaddition of a donor–acceptor (don–acc) cyclopropane and piperonal succinctly provides the core of virgatusin in a selective, high-yielding manner.