Combination of a binaphthol-derived phosphite and a C1-symmetric phosphinamine generates heteroleptic catalysts in Rh- and Pd-mediated reactions

Luca Pignataro; Benita Lynikaite; Raffaele Colombo; Stefano Carboni; Martin Krupička; Umberto Piarulli; Cesare Gennari

doi:10.1039/B908167D

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Chemical Communications

Issue 24, 2009

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Combination of a binaphthol-derived phosphite and a C₁-symmetric phosphinamine generates heteroleptic catalysts in Rh- and Pd-mediated reactions

Luca Pignataro , Benita Lynikaite , Raffaele Colombo , Stefano Carboni , Martin Krupička , Umberto Piarulli and Cesare Gennari

Chem. Commun., 2009, 3539-3541

DOI: 10.1039/B908167D
Received 23 Apr 2009, Accepted 11 May 2009
First published on the web 21 May 2009
This article is part of the collection: Selective Catalysis for Organic Synthesis

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Abstract
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Heteroleptic complexes, formed selectively by using a 1 : 1 combination of a σ-donor and a π-acceptor ligand, are involved in Rh- and Pd-catalysed reactions.

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Supplementary Info

Experimental procedures, characterisation data for all newcompounds, complexation experiments (along with copies of ³¹P- and ¹H-NMR spectra), full screening of the ligands in theRh- and Pd-catalysed reactions, and details of the DFTcalculations
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Luca Pignataro
Benita Lynikaite
Raffaele Colombo
Stefano Carboni
Martin Krupička
Umberto Piarulli
Cesare Gennari

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Chemical Communications

Combination of a binaphthol-derived phosphite and a C₁-symmetric phosphinamine generates heteroleptic catalysts in Rh- and Pd-mediated reactions

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