Bonding mode of a new bis-phosphine-borane alkyl ligand to a Rh(I) species

Matthias Blug; Dan Grünstein; Gilles Alcaraz; Sylviane Sabo-Etienne; Xavier-Frederic Le Goff; Pascal Le Floch; Nicolas Mézailles

doi:10.1039/B907813D

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Chemical Communications

Issue 29, 2009

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Bonding mode of a new bis-phosphine-borane alkyl ligand to a Rh(I) species

Matthias Blug , Dan Grünstein , Gilles Alcaraz , Sylviane Sabo-Etienne , Xavier-Frederic Le Goff , Pascal Le Floch and Nicolas Mézailles

Chem. Commun., 2009, 4432-4434

DOI: 10.1039/B907813D
Received 17 Apr 2009, Accepted 27 May 2009
First published on the web 11 Jun 2009

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Abstract
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The stoichiometric reaction of [Rh(COD)Cl]₂ with the anion resulting from the deprotonation of dppm(BH₃)₂ yielded a new alkyl Rh(I) complex; the coordination modes of the BH₃ groups are discussed on the basis of X-ray data, variable temperature multinuclear NMR experiments and DFT studies.

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Articles By

Matthias Blug
Dan Grünstein
Gilles Alcaraz
Sylviane Sabo-Etienne
Xavier-Frederic Le Goff
Pascal Le Floch
Nicolas Mézailles

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Chemical Communications

Bonding mode of a new bis-phosphine-borane alkyl ligand to a Rh(I) species

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