Azeotropic reflux
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Azeotropic reflux chromatography : an efficient solution to a difficult separation in the scale-up synthesis of spongistatin 1
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Department of Chemistry, University of Cambridge, Lensfield Road, Cambridge, UK
E-mail: mo263@cam.ac.uk ;
Fax: +44 (0) 1223 336442 ;
Tel: +44 (0) 1223 336398
E-mail: mo263@cam.ac.uk ;
Fax: +44 (0) 1223 336442 ;
Tel: +44 (0) 1223 336398
Org. Biomol. Chem., 2008,6, 1159-1164
DOI: 10.1039/B719569A
Received 19 Dec 2007, Accepted 25 Jan 2008
First published online 19 Feb 2008
Organic & Biomolecular Chemistry
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