Highly atom efficient aluminium triflate catalysed acetal formation

D. Bradley G. Williams; Michelle C. Lawton

doi:10.1039/B805748F

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Green Chemistry

Issue 9, 2008

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Highly atom efficient aluminium triflate catalysed acetal formation

D. Bradley G. Williams and Michelle C. Lawton

Green Chem., 2008, 10, 914-917

DOI: 10.1039/B805748F
Received 04 Apr 2008, Accepted 28 Jul 2008
First published on the web 05 Aug 2008

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Aromatic and aliphatic acetals are formed in excellent yields under solventless conditions at room temperature within 30 minutes by treating aldehydes and ketones with 0.5 mol% Al(OTf)₃ as a recyclable catalyst in the presence of only 1.2 equivalents of an orthoester as reagent.

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Literature references for known compounds prepared, analytical data and NMR spectra for new compounds
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