A chiral C3-symmetric hexanuclear triangular-prismatic copper(II) cluster derived from a highly modular dipeptidic N,N′-terephthaloyl-bis(S-aminocarboxylato) ligand

Barbara Wisser; Anne-Christine Chamayou; Robert Miller; Wolfgang Scherer; Christoph Janiak

doi:10.1039/B717207A

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CrystEngComm

Issue 5, 2008

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A chiral C₃-symmetric hexanuclear triangular-prismatic copper(II) cluster derived from a highly modular dipeptidic N,N′-terephthaloyl-bis(S-aminocarboxylato) ligand

Barbara Wisser , Anne-Christine Chamayou , Robert Miller , Wolfgang Scherer and Christoph Janiak

CrystEngComm, 2008, 10, 461-464

DOI: 10.1039/B717207A
Received 07 Nov 2007, Accepted 03 Jan 2008
First published on the web 23 Jan 2008

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The enantiomeric dipeptidic ligand N,N′-terephthaloyl-bis(L-phenylalaninato) (TBPhe^2–) reacts with copper(II) acetate in ethanol under the formation of the hexanuclear double-layered triangular-prismatic cluster [Cu₂(μ₄-TBPhe-κO:κO′:κO″:κO′″)₂(EtOH)(H₂O)]₃· [similar] 28(H₂O/0.33EtOH) with C₃-symmetry, homochiral conformer assembly in the crystal and strong antiferromagnetic coupling within the Cu₂(O₂CR)₄ paddle-wheel unit (J = −214 K).

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Barbara Wisser
Anne-Christine Chamayou
Robert Miller
Wolfgang Scherer
Christoph Janiak

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CrystEngComm

A chiral C₃-symmetric hexanuclear triangular-prismatic copper(II) cluster derived from a highly modular dipeptidic N,N′-terephthaloyl-bis(S-aminocarboxylato) ligand

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