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Issue 44, 2008
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Deuterated polymer gels for measuring anisotropic NMR parameters with strongly reduced artefacts

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Abstract

Perdeuterated poly(styrene) is introduced as an almost artefact-free and arbitrarily scalable alignment medium for measuring residual dipolar couplings and other anisotropic NMR parameters; the spectral quality achievable in this new medium is demonstrated for HSQC spectra leading to the conformational analysis of staurosporine and homonuclear TOCSY-type experiments.

Graphical abstract: Deuterated polymer gels for measuring anisotropic NMR parameters with strongly reduced artefacts

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Publication details

The article was received on 25 Jul 2008, accepted on 03 Sep 2008 and first published on 06 Oct 2008


Article type: Communication
DOI: 10.1039/B812905C
Citation: Chem. Commun., 2008,0, 5722-5724
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    Deuterated polymer gels for measuring anisotropic NMR parameters with strongly reduced artefacts

    G. Kummerlöwe, S. Knör, A. O. Frank, T. Paululat, H. Kessler and B. Luy, Chem. Commun., 2008, 0, 5722
    DOI: 10.1039/B812905C

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