Photoactivatable HNO-releasing compounds using the retro-Diels–Alder reaction

Yusuke Adachi; Hidehiko Nakagawa; Kazuya Matsuo; Takayoshi Suzuki; Naoki Miyata

doi:10.1039/B811985F

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Chemical Communications

Issue 41, 2008

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Photoactivatable HNO-releasing compounds using the retro-Diels–Alder reaction

Yusuke Adachi , Hidehiko Nakagawa , Kazuya Matsuo , Takayoshi Suzuki and Naoki Miyata

Chem. Commun., 2008, 5149-5151

DOI: 10.1039/B811985F
Received 14 Jul 2008, Accepted 02 Sep 2008
First published on the web 23 Sep 2008

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Abstract
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We synthesized hetero-Diels–Alder cycloadducts from acyl nitroso derivatives and 9,10-dimethylanthracene, to be photo-inducible HNO-releasing agents and found that introduction of conjugated nitroaromatic groups effectively enhanced the responsiveness of HNO release to UV-A irradiation; we confirmed photoinduced HNO formation by EPR and GCMS analysis.

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Supplementary Info

Details of the synthesis of 1–6 and results of H-NMR and UV/Visanalysis
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Results of EPR, and GC analysis
PDF (616K)
Results of H-NMR analysis
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Yusuke Adachi
Hidehiko Nakagawa
Kazuya Matsuo
Takayoshi Suzuki
Naoki Miyata

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Chemical Communications

Photoactivatable HNO-releasing compounds using the retro-Diels–Alder reaction

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