A general approach to triphenylenes and azatriphenylenes: total synthesis of dehydrotylophorine and tylophorine

Andrew McIver; Douglas D. Young; Alexander Deiters

doi:10.1039/B811068A

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Chemical Communications

Issue 39, 2008

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A general approach to triphenylenes and azatriphenylenes: total synthesis of dehydrotylophorine and tylophorine

Andrew McIver , Douglas D. Young and Alexander Deiters

Chem. Commun., 2008, 4750-4752

DOI: 10.1039/B811068A
Received 30 Jun 2008, Accepted 16 Jul 2008
First published on the web 27 Aug 2008

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A convergent and flexible synthesis of substituted triphenylenes, azatriphenylenes, and the cytotoxic alkaloids dehydrotylophorine and tylophorine has been developed.

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General cyclotrimerization protocol and analytical data aswell as ¹H NMR spectra for compounds 3–4, 6–17, and 20–21
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Chemical Communications

A general approach to triphenylenes and azatriphenylenes: total synthesis of dehydrotylophorine and tylophorine

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