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Issue 39, 2008
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Diaryl ether synthesis in supercritical carbon dioxide in batch and continuous flow modes

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Abstract

A high yielding, batch mode synthesis of diaryl ethers and sulfides by an SNAr fluoride-mediated process in scCO2 has been developed; the use of a polymer-supported imidazolium fluoride reagent in batch mode led to the development of a fixed-bed continuous flow process, with high conversions.

Graphical abstract: Diaryl ether synthesis in supercritical carbon dioxide in batch and continuous flow modes

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Publication details

The article was received on 19 May 2008, accepted on 27 Jun 2008 and first published on 06 Aug 2008


Article type: Communication
DOI: 10.1039/B808374F
Citation: Chem. Commun., 2008,0, 4780-4782
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    Diaryl ether synthesis in supercritical carbon dioxide in batch and continuous flow modes

    J. Lee, M. J. Fuchter, R. M. Williamson, G. A. Leeke, E. J. Bush, I. F. McConvey, S. Saubern, J. H. Ryan and A. B. Holmes, Chem. Commun., 2008, 0, 4780
    DOI: 10.1039/B808374F

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