An improved method for the synthesis of zirconium (CCC-N-heterocyclic carbene) pincer complexes and applications in hydroamination

Joon Cho; T. Keith Hollis; Theodore R. Helgert; Edward J. Valente

doi:10.1039/B805174G

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Chemical Communications

Issue 40, 2008

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An improved method for the synthesis of zirconium (CCC-N-heterocyclic carbene) pincer complexes and applications in hydroamination

Joon Cho , T. Keith Hollis , Theodore R. Helgert and Edward J. Valente

Chem. Commun., 2008, 5001-5003

DOI: 10.1039/B805174G
Received 11 Apr 2008, Accepted 13 Aug 2008
First published on the web 19 Sep 2008

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Upon heating Zr(NMe₂)₄, 1,3-bis(N-butyl-imidazolium)benzene diiodide and toluene analytically pure Zr pincer complex was obtained, which was found to be an intramolecular hydroamination catalyst.

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Chemical Communications

An improved method for the synthesis of zirconium (CCC-N-heterocyclic carbene) pincer complexes and applications in hydroamination

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