The first side-on bound metal complex of diazene, HNNH

Leslie D. Field; Hsiu L. Li; Scott J. Dalgarno; Peter Turner

doi:10.1039/B802039F

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Chemical Communications

Issue 14, 2008

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The first side-on bound metal complex of diazene, HNNH

Leslie D. Field , Hsiu L. Li , Scott J. Dalgarno and Peter Turner

Chem. Commun., 2008, 1680-1682

DOI: 10.1039/B802039F
Received 05 Feb 2008, Accepted 18 Feb 2008
First published on the web 07 Mar 2008

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Abstract
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The side-on bound metal complex of diazene cis-[Fe(NH [double bond, length as m-dash] NH)(dmpe)₂] 2 was synthesised by reaction of [Fe(dmpe)₂Cl₂] with hydrazine in the presence of potassium graphite and characterised by ¹⁵N NMR spectroscopy and X-ray crystallography.

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Experimental conditions and spectroscopic details for 1–3
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Crystal structure data
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Chemical Communications

The first side-on bound metal complex of diazene, HNNH

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