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Issue 18, 2008
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Clean and efficient synthesis of O-silylcarbamates and ureas in supercritical carbon dioxide

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Abstract

The synthesis of a family of O-silylcarbamates from the corresponding silylamines has been achieved simply by heating the silylamine in supercritical carbon dioxide (scCO2), and these O-silylcarbamates have been shown to be effective precursors for the synthesis of a range of symmetrical and unsymmetrical ureas.

Graphical abstract: Clean and efficient synthesis of O-silylcarbamates and ureas in supercritical carbon dioxide

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Publication details

The article was received on 28 Jan 2008, accepted on 28 Feb 2008 and first published on 02 Apr 2008


Article type: Communication
DOI: 10.1039/B801537F
Citation: Chem. Commun., 2008,0, 2152-2154
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    Clean and efficient synthesis of O-silylcarbamates and ureas in supercritical carbon dioxide

    M. J. Fuchter, C. J. Smith, M. W. S. Tsang, A. Boyer, S. Saubern, J. H. Ryan and A. B. Holmes, Chem. Commun., 2008, 0, 2152
    DOI: 10.1039/B801537F

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