Accurate non-invasive determination of pKa of surface functionalised ion exchange monoliths using capacitively coupled contactless conductivity detection

Eoin Gillespie; Damian Connolly; Pavel N. Nesterenko; Brett Paull

doi:10.1039/B803349H

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Analyst

Issue 7, 2008

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Accurate non-invasive determination of pK_a of surface functionalised ion exchange monoliths using capacitively coupled contactless conductivity detection

Eoin Gillespie , Damian Connolly , Pavel N. Nesterenko and Brett Paull

Analyst, 2008, 133, 874-876

DOI: 10.1039/B803349H
Received 26 Feb 2008, Accepted 27 Mar 2008
First published on the web 03 Apr 2008

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Abstract
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Compounds
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The use of on-column capacitively coupled contactless conductivity detection for the accurate non-invasive visualisation of the pH dependence of covalently bound boronic acid groups within a monolithic polymeric capillary column is demonstrated.

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Reagents and instrumentation; simplified synthetic approach to boronic acid functionalisation
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Accurate non-invasive determination of pK_a of surface functionalised ion exchange monoliths using capacitively coupled contactless conductivity detection

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