Polymer supported naphthalene-catalysed sodium reactions

Tania R. van den Ancker; Cameron J. Love

doi:10.1039/B710308E

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Organic & Biomolecular Chemistry

Issue 21, 2007

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Polymer supported naphthalene-catalysed sodium reactions

Tania R. van den Ancker and Cameron J. Love

Org. Biomol. Chem., 2007, 5, 3520-3523

DOI: 10.1039/B710308E
Received 06 Jul 2007, Accepted 13 Sep 2007
First published on the web 20 Sep 2007

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Arene-catalysed sodium reactions have been utilised in the generation of organosodium complexes, from a variety of organochloride complexes, in high yield. Phenyltrimethylsilane, benzene and 2-methyl-1-phenyl-1-propanol were prepared in yields >80%, using polymer supported naphthalene-catalysed sodium reactions, whereby phenylsodium, prepared from the reaction of chlorobenzene, sodium powder and polymer-supported naphthalene (5–100%), was quenched with chlorotrimethylsilane, water or PrⁱCHO respectively.

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Organic & Biomolecular Chemistry

Polymer supported naphthalene-catalysed sodium reactions

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