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Issue 10, 2007
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Tagged phosphine reagents to assist reaction work-up by phase-switched scavenging using a modular flow reactor

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Abstract

The use of three orthogonally tagged phosphine reagents to assist chemical work-up via phase-switch scavenging in conjunction with a modular flow reactor is described. These techniques (acidic, basic and Click chemistry) are used to prepare various amides and tri-substituted guanidines from in situ generated iminophosphoranes.

Graphical abstract: Tagged phosphine reagents to assist reaction work-up by phase-switched scavenging using a modular flow reactor

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Publication details

The article was received on 28 Feb 2007, accepted on 19 Mar 2007 and first published on 16 Apr 2007


Article type: Paper
DOI: 10.1039/B703033A
Citation: Org. Biomol. Chem., 2007,5, 1562-1568
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    Tagged phosphine reagents to assist reaction work-up by phase-switched scavenging using a modular flow reactor

    C. D. Smith, I. R. Baxendale, G. K. Tranmer, M. Baumann, S. C. Smith, R. A. Lewthwaite and S. V. Ley, Org. Biomol. Chem., 2007, 5, 1562
    DOI: 10.1039/B703033A

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