Design, characterization, and X-ray structure of an interlocked dinuclear chair-like metallomacrocycle: [FeII2(3,5-bis(2,2′:6′,2″-terpyridin-4′-phen-3-yl)toluene)2][4PF6−]

Ibrahim Eryazici; Pingshan Wang; Charles N. Moorefield; Matthew Panzer; Semih Durmus; Carol D. Shreiner; George R. Newkome

doi:10.1039/B616014J

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Design, characterization, and X-ray structure of an interlocked dinuclear chair-like metallomacrocycle: [Fe^II₂(3,5-bis(2,2′:6′,2″-terpyridin-4′-phen-3-yl)toluene)₂][4PF₆⁻]†

Ibrahim Eryazici,^a Pingshan Wang,^a Charles N. Moorefield,^c Matthew Panzer,^b Semih Durmus,^b Carol D. Shreiner^a and George R. Newkome*^ab

Author affiliations

* Corresponding authors

^a Department of Polymer Science, The University of Akron, Akron, OH, USA
E-mail: newkome@uakron.edu
Fax: +1 330 972 2413
Tel: +1 330 972 6458

^b Department of Chemistry, The University of Akron, Akron, OH, USA

^c Maurice Morton Institute of Polymer Science, The University of Akron, Akron, OH, USA

Abstract

The self-assembly of 3,5-bis(2,2′:6′,2″-terpyridin-4′-phen-3-yl)toluene with an equimolar amount of a Fe^II salt afforded a high yield of an interlocked dinuclear tetracationic “molecular gear” that was confirmed by single crystal X-ray data.

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Supplementary files

Crystal structure data TXT (29K)

Article information

DOI: https://doi.org/10.1039/B616014J
Article type: Communication
Submitted: 03 Nov 2006
Accepted: 20 Dec 2006
First published: 09 Jan 2007

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Dalton Trans., 2007, 626-628

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Design, characterization, and X-ray structure of an interlocked dinuclear chair-like metallomacrocycle: [Fe^II₂(3,5-bis(2,2′:6′,2″-terpyridin-4′-phen-3-yl)toluene)₂][4PF₆⁻]

I. Eryazici, P. Wang, C. N. Moorefield, M. Panzer, S. Durmus, C. D. Shreiner and G. R. Newkome, Dalton Trans., 2007, 626 DOI: 10.1039/B616014J

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Dalton Transactions