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Issue 10, 2007
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Solvent effect in a “solvent free” reaction

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Vapour digestion of a mixture of solid [Fe(η5-C5H4–C5H4N)2] and solid pimelic acid HOOC(CH2)5COOH in the presence of solvent vapours generates co-crystals of different stoichiometry depending on the protic or aprotic nature of the solvent. The nature of the products has been ascertained by a combined use of SSNMR and X-ray diffraction.

Graphical abstract: Solvent effect in a “solvent free” reaction

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The article was received on 03 Aug 2007, accepted on 03 Aug 2007 and first published on 20 Aug 2007

Article type: Communication
DOI: 10.1039/B711983F
Citation: CrystEngComm, 2007,9, 879-881
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    Solvent effect in a “solvent free” reaction

    D. Braga, S. L. Giaffreda, F. Grepioni, M. R. Chierotti, R. Gobetto, G. Palladino and M. Polito, CrystEngComm, 2007, 9, 879
    DOI: 10.1039/B711983F

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