Uranyl stabilized Schiff base complex

Mohan S. Bharara; Stephen A. Tonks; Anne E. V. Gorden

doi:10.1039/B712322A

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Chemical Communications

Issue 39, 2007

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Uranyl stabilized Schiff base complex

Mohan S. Bharara , Stephen A. Tonks and Anne E. V. Gorden

Chem. Commun., 2007, 4006-4008

DOI: 10.1039/B712322A
Received 10 Aug 2007, Accepted 09 Sep 2007
First published on the web 14 Sep 2007

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Abstract
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Uranyl Schiff base complex [(UO₂)₂(Salpro)(OH)(Solvent)₂] (1) in the presence of excess of ethylenediamine (EDA) does not undergo nucleophilic addition (hydrolysis) and substitution (transamination) reactions due to an extended chelation [2N, 3O + OH] by the flexible backbone.

Supplementary Info

Experimental procedure, NMR and mass spectra, structure of SalproH ₃, crystal data, selected bond distances and angles
PDF (345K)
Crystal structure data
TXT (67K)
¹H NMR of 1 in DMSO
JPG (2361K)
¹³C NMR of 1 in DMSO
JPG (2334K)
Mass spectrum of 1·(MeOH) ₂
JPG (2067K)
Mass spectrum of 2·MeOH
JPG (2229K)

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Uranyl stabilized Schiff base complex

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