Cobalt-catalyzed intermolecular C–H amination with bromamine-T as nitrene source

Jeremiah D. Harden; Joshua V. Ruppel; Guang-Yao Gao; X. Peter Zhang

doi:10.1039/B710677G

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Chemical Communications

Issue 44, 2007

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Cobalt-catalyzed intermolecular C–H amination with bromamine-T as nitrene source

Jeremiah D. Harden , Joshua V. Ruppel , Guang-Yao Gao and X. Peter Zhang

Chem. Commun., 2007, 4644-4646

DOI: 10.1039/B710677G
Received 12 Jul 2007, Accepted 22 Aug 2007
First published on the web 03 Sep 2007

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Abstract
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Cobalt, supported by porphyrin ligands, is capable of catalyzing intermolecular nitrene insertion of sp³ C–H bonds with bromamine-T as the nitrene source, forming the desired tosyl-protected amines with NaBr as the by-product.

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Supplementary Info

Full experimental procedures for the synthesis of compounds 2a– f, their characterization data and ¹H NMR spectra
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Chemical Communications

Cobalt-catalyzed intermolecular C–H amination with bromamine-T as nitrene source

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