Synthesis of para-methoxybenzyl (PMB) ethers under neutral conditions

Ernest O. Nwoye; Gregory B. Dudley

doi:10.1039/B617926F

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Chemical Communications

Issue 14, 2007

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Synthesis of para-methoxybenzyl (PMB) ethers under neutral conditions

Ernest O. Nwoye and Gregory B. Dudley

Chem. Commun., 2007, 1436-1437

DOI: 10.1039/B617926F
Received 08 Dec 2006, Accepted 13 Feb 2007
First published on the web 26 Feb 2007

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2-(4-Methoxybenzyloxy)-4-methylquinoline reacts with methyl triflate in the presence of alcohols to generate a neutral organic salt that transfers the para-methoxybenzyl (PMB) protecting group onto alcohols in high yield and under mild conditions.

Abstract from Methods in Organic Synthesis 2007

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Chemical Communications

Synthesis of para-methoxybenzyl (PMB) ethers under neutral conditions

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