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Issue 12, 2007
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First hypervalent iodine(III)-catalyzed C–N bond forming reaction: catalytic spirocyclization of amides to N-fused spirolactams

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Abstract

A protic solvent, 2,2,2-trifluoroethanol (CF3CH2OH), was successfully introduced into hypervalent iodine(III)-involved catalytic cycles as an effective solvent, and the first iodoarene-catalyzed intramolecular carbon–nitrogen bond forming reaction was achieved under strong acid-free and mild conditions.

Graphical abstract: First hypervalent iodine(iii)-catalyzed C–N bond forming reaction: catalytic spirocyclization of amides to N-fused spirolactams

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Publication details

The article was received on 13 Nov 2006, accepted on 28 Nov 2006 and first published on 22 Dec 2006


Article type: Communication
DOI: 10.1039/B616510A
Citation: Chem. Commun., 2007,0, 1224-1226
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    First hypervalent iodine(III)-catalyzed C–N bond forming reaction: catalytic spirocyclization of amides to N-fused spirolactams

    T. Dohi, A. Maruyama, Y. Minamitsuji, N. Takenaga and Y. Kita, Chem. Commun., 2007, 0, 1224
    DOI: 10.1039/B616510A

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