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Issue 48, 2006
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Sequential one-pot bimetallic Ir(III)/Pd(0) catalysed mono-/bis-alkylation and spirocyclisation processes of 1,3-dimethylbarbituric acid and allenes

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Abstract

Microwave assisted indirect functionalization of alcohols with 1,3-dimethylbarbituric acid followed by spirocyclisation employing a sequential one-pot Ir(III)/Pd(0) catalysed process, involving the formation of three new C–C bonds, one spirocyclic ring and one di- or tri-substituted exocyclic alkene, is described.

Graphical abstract: Sequential one-pot bimetallic Ir(iii)/Pd(0) catalysed mono-/bis-alkylation and spirocyclisation processes of 1,3-dimethylbarbituric acid and allenes

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Publication details

The article was received on 28 Sep 2006, accepted on 27 Oct 2006 and first published on 15 Nov 2006


Article type: Communication
DOI: 10.1039/B614098J
Citation: Chem. Commun., 2006,0, 5000-5002
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    Sequential one-pot bimetallic Ir(III)/Pd(0) catalysed mono-/bis-alkylation and spirocyclisation processes of 1,3-dimethylbarbituric acid and allenes

    C. Löfberg, R. Grigg, A. Keep, A. Derrick, V. Sridharan and C. Kilner, Chem. Commun., 2006, 0, 5000
    DOI: 10.1039/B614098J

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