Issue 34, 2006
From the journal:

Chemical Communications

Real-time monitoring of microwave-promoted organometallic ligand-substitution reactions using in situ Raman spectroscopy†

Thomas M. Barnarda  and  Nicholas E. Leadbeater*b  

* Corresponding authors

a CEM Microwave Technology, 3100 Smith Farm Road, Matthews, NC 28104, USA
E-mail: mike.barnard@cem.com
Fax: +1 704 821-7894
Tel: +1 704 821-7015

b Department of Chemistry, University of Connecticut, 55 North Eagleville Road, Storrs, CT 06269-3060, USA
E-mail: nicholas.leadbeater@uconn.edu
Fax: +1 860 486 2981
Tel: +1 860 486 5076

Abstract

An apparatus has been developed for real-time monitoring of organometallic reactions under microwave irradiation using in situ Raman spectroscopy and its application for monitoring ligand substitution reactions of Mo(CO)6 demonstrated.

Graphical abstract: Real-time monitoring of microwave-promoted organometallic ligand-substitution reactions using in situ Raman spectroscopy

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Article information

DOI
https://doi.org/10.1039/B608793K
Article type
Communication
Submitted
20 Jun 2006
Accepted
12 Jul 2006
First published
01 Aug 2006

Chem. Commun., 2006, 3615-3616

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Real-time monitoring of microwave-promoted organometallic ligand-substitution reactions using in situ Raman spectroscopy

T. M. Barnard and N. E. Leadbeater, Chem. Commun., 2006, 3615 DOI: 10.1039/B608793K

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