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Issue 4, 2006
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Supramolecular stabilization of hydroxylamine TEMPOH by complexation with an amphiphilic calixarene

Gennady S. Ananchenko,*a  Michaela Pojarova,a  Konstantin A. Udachin,a  Donald M. Leek,a  Antony W. Colemanb  and  John A. Ripmeestera 
Author affiliations

* Corresponding authors

a NRC Steacie Institute for Molecular Sciences, 100 Sussex Drive, Ottawa, Canada
E-mail: Gennady.Ananchenko@nrc-cnrc.gc.ca
Fax: (+1) 613 998 7833
Tel: (+1) 613 993 2372

b Institut de Chimie et Biologie des Proteins, 7 Passage du Vercors, Lyon Cedex 07, France

Abstract

In an ethanol/water mixture, the nitroxyl radical TEMPO abstracts a hydrogen atom from a phenolic OH group of the amphiphilic para-hexanoylcalix[4]arene, and the hydroxylamine TEMPOH formed yields a stable inclusion complex with another molecule of the calixarene.

Graphical abstract: Supramolecular stabilization of hydroxylamine TEMPOH by complexation with an amphiphilic calixarene

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Publication details

The article was received on 18 Aug 2005, accepted on 03 Nov 2005 and first published on 07 Dec 2005


Article type: Communication
DOI: 10.1039/B511810G
Citation: Chem. Commun., 2006,0, 386-388
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    Supramolecular stabilization of hydroxylamine TEMPOH by complexation with an amphiphilic calixarene

    G. S. Ananchenko, M. Pojarova, K. A. Udachin, D. M. Leek, A. W. Coleman and J. A. Ripmeester, Chem. Commun., 2006, 0, 386
    DOI: 10.1039/B511810G

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