Pictet–Spengler reactions in multiphasic supercritical carbon dioxide/CO2-expanded liquid media. In situ generation of carbamates as a strategy for reactions of amines in supercritical carbon dioxide

Joshua R. Dunetz; Rocco P. Ciccolini; Morgan Fröling; Scott M. Paap; Andrew J. Allen; Andrew B. Holmes; Jefferson W. Tester; Rick L. Danheiser

doi:10.1039/B508151C

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Chemical Communications

Issue 35, 2005

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Pictet–Spengler reactions in multiphasic supercritical carbon dioxide/CO₂-expanded liquid media. In situ generation of carbamates as a strategy for reactions of amines in supercritical carbon dioxide

Joshua R. Dunetz , Rocco P. Ciccolini , Morgan Fröling , Scott M. Paap , Andrew J. Allen , Andrew B. Holmes , Jefferson W. Tester and Rick L. Danheiser

Chem. Commun., 2005, 4465-4467

DOI: 10.1039/B508151C
Received 08 Jun 2005, Accepted 06 Jul 2005
First published on the web 04 Aug 2005

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Acyl-Pictet–Spengler cyclizations can be achieved in scCO₂/CO₂-expanded liquid media via the in situ formation of carbamate derivatives of β-arylethylamines.

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Description of reaction apparatus and experimental procedures and characterization data for 14? 21 and 24.
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Joshua R. Dunetz
Rocco P. Ciccolini
Morgan Fröling
Scott M. Paap
Andrew J. Allen
Andrew B. Holmes
Jefferson W. Tester
Rick L. Danheiser

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Chemical Communications

Pictet–Spengler reactions in multiphasic supercritical carbon dioxide/CO₂-expanded liquid media. In situ generation of carbamates as a strategy for reactions of amines in supercritical carbon dioxide

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