[PtMe(iPr3P)2]+: a Pt(II) complex with an agostic interaction that undergoes C–H activation

Michael J. Ingleson; Mary F. Mahon; Andrew S. Weller

doi:10.1039/B410846A

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Chemical Communications

Issue 21, 2004

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[PtMe(ⁱPr₃P)₂]⁺: a Pt(II) complex with an agostic interaction that undergoes C–H activation

Michael J. Ingleson,*^a Mary F. Mahon^a and Andrew S. Weller*^a

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Department of Chemistry, University of Bath, Bath, UK
E-mail: a.s.weller@bath.ac.uk ;
Fax: +44 (0)1225 386231 ;
Tel: +44 (0)1225 383394

Chem. Commun., 2004, 2398-2399

DOI: 10.1039/B410846A
Received 16 Jul 2004, Accepted 11 Aug 2004
First published online 23 Sep 2004

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Abstract
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The T-shaped Pt(II) complex [PtMe(ⁱPr₃P)₂][1-H-closo-CB₁₁Me₁₁], which is stabilised by an agostic interaction, undergoes acid-catalysed intramolecular C–H activation in the presence of THF to afford cyclometallated [Pt(THF)(ⁱPr₃P)(ⁱPr₂PCHMeCH₂)][1-H-closo-CB₁₁Me₁₁].

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Experimental data, DFT calculations and proposed mechanism for the formation of 3
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