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Issue 24, 2003
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Synthesis of the cyclobutanone core of solanoeclepin A via intramolecular allene butenolide photocycloaddition

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Abstract

The compact tricyclic substructure of solanoeclepin A containing the cyclobutanone ring was prepared by using as the key step a highly regioselective intramolecular [2 + 2]-photocycloaddition reaction between one of the π-bonds of an allene and the CC double bond of a butenolide.

Graphical abstract: Synthesis of the cyclobutanone core of solanoeclepin A via intramolecular allene butenolide photocycloaddition

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Publication details

The article was received on 24 Sep 2003, accepted on 23 Oct 2003 and first published on 29 Oct 2003


Article type: Communication
DOI: 10.1039/B311415E
Citation: Org. Biomol. Chem., 2003,1, 4364-4366
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    Synthesis of the cyclobutanone core of solanoeclepin A via intramolecular allene butenolide photocycloaddition

    B. T. B. Hue, J. Dijkink, S. Kuiper, K. K. Larson, F. S. Guziec, Jr., K. Goubitz, J. Fraanje, H. Schenk, J. H. van Maarseveen and H. Hiemstra, Org. Biomol. Chem., 2003, 1, 4364
    DOI: 10.1039/B311415E

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