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Issue 22, 2003
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Using a novel plug flow reactor for the in situ, simultaneous, monitoring of SAXS and WAXD during crystallisation from solution

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Abstract

The design and application of a novel plug flow crystalliser is described. Simultaneous collection of SAXS and WAXD during the nucleation and crystal growth of a small organic molecule from solution is reported. Preliminary data imply the separation of a non-diffracting phase prior to the appearance of crystalline solid.

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Publication details

The article was received on 04 Aug 2003, accepted on 03 Oct 2003 and first published on 14 Oct 2003


Article type: Communication
DOI: 10.1039/B309309C
Citation: Phys. Chem. Chem. Phys., 2003,5, 4998-5000
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    Using a novel plug flow reactor for the in situ, simultaneous, monitoring of SAXS and WAXD during crystallisation from solution

    H. G. Alison, R. J. Davey, J. Garside, M. J. Quayle, G. J. T. Tiddy, D. T. Clarke and G. R. Jones, Phys. Chem. Chem. Phys., 2003, 5, 4998
    DOI: 10.1039/B309309C

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