Synthesis of neutral nickel catalysts for ethylene polymerization – the influence of ligand size on catalyst stability

Eric F. Connor; Todd R. Younkin; Jason I. Henderson; Andrew W. Waltman; Robert H. Grubbs

doi:10.1039/B306701G

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Chemical Communications

Issue 18, 2003

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Synthesis of neutral nickel catalysts for ethylene polymerization – the influence of ligand size on catalyst stability

Eric F. Connor,^a Todd R. Younkin,^a Jason I. Henderson,^a Andrew W. Waltman^a and Robert H. Grubbs*^a

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Division of Chemistry and Chemical Engineering, Arnold and Mabel Beckman Laboratories of Chemical Synthesis, California Institute of Technology, Pasadena, California 91125

Chem. Commun., 2003, 2272-2273

DOI: 10.1039/B306701G
Received 12 Jun 2003, Accepted 30 Jul 2003
First published online 15 Aug 2003

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Abstract
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A facile synthesis of nickel salicylaldimine complexes with labile dissociating ligands is described. In addition to producing highly active ethylene polymerization catalysts, important insights into the effect of ligand size on catalyst stability and information on the mechanism of polymerization are provided.

Abstract from Catalysts & Catalysed Reactions 2004

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Supplementary Info

¹Experimental protocol for (tmeda)Ni(Me) ₂ and compounds 3, 4, 7 - 10
DOC (328K)
¹H-NMR magnetization transfer data for compound 7
PDF (45K)
Crystal structure data
TXT (100K)

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Eric F. Connor
Todd R. Younkin
Jason I. Henderson
Andrew W. Waltman
Robert H. Grubbs

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Chemical Communications

Synthesis of neutral nickel catalysts for ethylene polymerization – the influence of ligand size on catalyst stability

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