Synthesis and structure of [{Sn(μ–PCy)}3(Na·PMDETA)2], containing an electron-deficient [{Sn(μ–PCy)}3]2− dianion

Paula Alvarez-Bercedo; Andrew D. Bond; Robert Haigh; Alexander D. Hopkins; Gavin T. Lawson; Mary McPartlin; David Moncrieff; Marta E. Gonzalez Mosquera; Jeremy M. Rawson; Anthony D. Woods; Dominic S. Wright

doi:10.1039/B300522D

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Chemical Communications

Issue 11, 2003

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Synthesis and structure of [{Sn(μ–PCy)}₃(Na·PMDETA)₂], containing an electron-deficient [{Sn(μ–PCy)}₃]²⁻ dianion

Paula Alvarez-Bercedo,^a Andrew D. Bond,^a Robert Haigh,^a Alexander D. Hopkins,^a Gavin T. Lawson,^a Mary McPartlin,^b David Moncrieff,^c Marta E. Gonzalez Mosquera,^d Jeremy M. Rawson,^a Anthony D. Woods^a and Dominic S. Wright*^a

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Chemistry Department, Cambridge University, Lensfield Road, UK
E-mail: dsw1000@cus.cam.ac.uk ;
Fax: [+44] (0)1223 336362 ;
Tel: [+44] (0)1223 763122

School of Chemistry, University of North London, UK

School of Computational Science & Information Technology, Florida State University, Tallahassee, USA

Department of Organic and Inorganic Chemistry, Universidad de Oviedo, Spain

Chem. Commun., 2003, 1288-1289

DOI: 10.1039/B300522D
Received 15 Jan 2003, Accepted 07 Apr 2003
First published online 06 May 2003

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The reaction of CyPHNa with Sn(NMe₂)₂ in the presence of PMDETA (= {Me₂NCH₂CH₂}₂NMe) gives the title compound [{Sn(μ–PCy)}₃(Na·PMDETA)₂] (1), containing an electron-deficient [(Sn(μ–PCy)}]₃²⁻ dianion with a novel two-electron, three centre (2e–3c) bonding arrangement.

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Chemical Communications

Synthesis and structure of [{Sn(μ–PCy)}₃(Na·PMDETA)₂], containing an electron-deficient [{Sn(μ–PCy)}₃]²⁻ dianion

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Chemical Communications

Synthesis and structure of [{Sn(μ–PCy)}3(Na·PMDETA)2], containing an electron-deficient [{Sn(μ–PCy)}3]2− dianion

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Synthesis and structure of [{Sn(μ–PCy)}₃(Na·PMDETA)₂], containing an electron-deficient [{Sn(μ–PCy)}₃]²⁻ dianion