In this communication we report the synthesis and structural characterisation of a new body centred polymorph of Cu2WS4 prepared using hydrothermal methods. I–Cu2WS4 crystallises in space group I![[4 with combining macron]](https://www.rsc.org/images/entities/char_0034_0304.gif)
2m with cell parameters a
=
b
= 5.44427(8), c
= 10.0687(2)
Å and has a new structure type containing layers of edge-sharing CuS4 and WS4 tetrahedra.
C. J. Crossland and J. S. O. Evans, Chem. Commun., 2003, 2292 DOI: 10.1039/B306633A
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