Chemical sequential extraction for metal partitioning in environmental solid samples.

A. V. Filgueiras; I. Lavilla; C. Bendicho

doi:10.1039/B207574C

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Journal of Environmental Monitoring

Issue 6, 2002

Cutting-Edge Research on Environmental Processes & Impacts

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Chemical sequential extraction for metal partitioning in environmental solid samples.

A. V. Filgueiras,^a I. Lavilla^a and C. Bendicho*^a

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Departamento de Química Analítica y Alimentaria, Area de Química Analítica, Facultad de Ciencias (Química), Universidad de Vigo, As Lagoas-Marcosende s/n, 36200 Vigo, Spain
E-mail: bendicho@uvigo.es

J. Environ. Monit., 2002,4, 823-857

DOI: 10.1039/B207574C
Received 02 Aug 2002, Accepted 20 Sep 2002
First published online 16 Oct 2002

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Abstract
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A comprehensive review of the sequential extraction schemes for metal fractionation in environmental samples (i.e., sediment, soil, sewage sludge, fly ash, etc.) is presented. The review contains more than 400 references and covers principally the literature published over the last decade. The use of each reagent involved in these schemes is looked at critically, and guidelines for their selectivity and extraction capacity are given. The operational character of these schemes is emphasised. Topics such as comparability between sequential extraction schemes of widespread use, harmonisation, acceleration, validation, etc. are addressed and future developments outlined.

Abstract from Analytical Abstracts 2003

A comprehensive review of the sequential extraction schemes for metal fractionation in environmental samples (i.e., sediment, soil, sewage sludge, fly ash, etc.) is presented. The review covers principally the literature published over the last decade. The use of each reagent involved in these schemes is looked at critically, and guidelines for their selectivity and extraction capacity are given. The operational character of these schemes is emphasised. Topics such as comparability between sequential extraction schemes of widespread use, harmonisation, acceleration, validation, etc., are addressed and future developments outlined. (434 references).

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