The first time-resolved in situ X-ray diffraction studies of the hydrothermal crystallisation of open-framework zinc phosphates reveal a pathway of sequential crystallisation involving formation of a metastable low dimensional chain phase before the growth of three-dimensional zeolitic architectures.
Direct in situ observation of increasing structural dimensionality during the hydrothermal formation of open-framework zinc phosphates
R. I. Walton, A. J. Norquist, S. Neeraj, S. Natarajan, C. N. R. Rao and D. O’Hare, Chem. Commun., 2001, 1990 DOI: 10.1039/B105659J
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