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Issue 5, 2000
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Microwave assisted preparation of binary oxide nanoparticles

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Abstract

A group of binary oxide nanophase materials were prepared using a microwave assisted soft-chemical route. BaTiO3, Ba6Ti17O40, BaZrO3 and PbTiO3 were prepared from BaCl2 hydrate, Pb(Ac)2, Ti(OPri)4 and ZrOCl2. All reactions were performed in ethylene glycol, which acted as both a solvent and a growth regulating agent, under atmospheric pressure in a microwave reactor. The products that were obtained were analyzed by using XRD, TEM, XPS, EDX and FT-IR.

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Publication details

The article was received on 04 Nov 1999, accepted on 03 Feb 2000 and first published on 29 Mar 2000


Article type: Paper
DOI: 10.1039/A908795H
Citation: J. Mater. Chem., 2000,10, 1251-1254
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    Microwave assisted preparation of binary oxide nanoparticles

    O. Palchik, J. Zhu and A. Gedanken, J. Mater. Chem., 2000, 10, 1251
    DOI: 10.1039/A908795H

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