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Issue 15, 1998
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Rare M7O2 double tetrahedral core in molecular species: preparation, structure and properties of [Zn7O2(O2CMe)10(1-Meim)2] (1-Meim = 1-methylimidazole)

Nikolia Lalioti,  Spyros P. Perlepes,  Evy Manessi-Zoupa,  Catherine P. Raptopoulou,  Aris Terzis,  Abil E. Aliev  and  Ioannis P. Gerothanassis 

Abstract

The 2:1 reaction between Zn(O2CMe)2·2H2O and 1-Meim in refluxing MeCN gives [Zn7O2(O2CMe)10(1-Meim)2] 1 which comprises two vertex-sharing tetranuclear Zn4(µ4-O)(η1: η1:µ2-O2CMe)5(1-Meim) units; solid-state 13C and 15N NMR spectra reveal structural details of the complex.

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Article type: Paper
DOI: 10.1039/A802844C
Citation: Chem. Commun., 1998,0, 1513-1514
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    Rare M7O2 double tetrahedral core in molecular species: preparation, structure and properties of [Zn7O2(O2CMe)10(1-Meim)2] (1-Meim = 1-methylimidazole)

    N. Lalioti, S. P. Perlepes, E. Manessi-Zoupa, C. P. Raptopoulou, A. Terzis, A. E. Aliev and I. P. Gerothanassis, Chem. Commun., 1998, 0, 1513
    DOI: 10.1039/A802844C

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