SCHEDULED MAINTENANCE
A new strategy for the construction of the isotwistane skeleton is reported from easily available cyclohexadienes which involves stereoselective alkylation of a bicyclooctenone derivative and a decarboxylative 5-exo-trig radical cyclisation as the key steps in the total synthesis of 5-epi-pupukean-2-one.
K. Kaliappan and G. S. R. Subba Rao, J. Chem. Soc., Perkin Trans. 1, 1997, 3387 DOI: 10.1039/A704312K
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