A terminal molybdenum carbide prepared by methylidyne deprotonation

Jonas C. Peters; Aaron L. Odom; Christopher C. Cummins

doi:10.1039/A704251E

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Chemical Communications

Issue 20, 1997

Urgent high quality communications from across the chemical sciences.

Impact Factor 6.169 100 Issues per Year Indexed in MEDLINE

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A terminal molybdenum carbide prepared by methylidyne deprotonation

Jonas C. Peters, Aaron L. Odom and Christopher C. Cummins

Chem. Commun., 1997, 1995-1996

DOI: 10.1039/A704251E

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Abstract
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The carbide anion [CMo{N(R)Ar}₃]^– [R = C(CD₃)₂CH₃, Ar = C₆H₃Me₂-3,5], is obtained by deprotonation of the corresponding methylidyne compound, [HCMo{N(R)Ar}₃], and is characterized by X-ray diffraction as its {K(benzo-15-crown-5)₂}⁺ salt, thereby providing precedent for the carbon atom as a terminal substituent in transition-metal chemistry.

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