Investigation of transport across an immiscible liquid/liquid interface. Electrochemical and second harmonic generation studies

Michael J. Crawford; Jeremy G. Frey; T. J. VanderNoot; Yuguang Zhao

doi:10.1039/FT9969201369

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Journal of the Chemical Society, Faraday Transactions

Issue 8, 1996

Journal of the Chemical Society, Faraday Transactions; was published from 1990 - 1998. In 1999 it merged with a number of European chemical society physical Chemistry journals to become Physical Chemistry Chemical Physics.

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Investigation of transport across an immiscible liquid/liquid interface. Electrochemical and second harmonic generation studies

Michael J. Crawford, Jeremy G. Frey, T. J. VanderNoot and Yuguang Zhao

J. Chem. Soc., Faraday Trans., 1996,92, 1369-1373

DOI: 10.1039/FT9969201369

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Abstract
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An electrochemical investigation of the transport of the crown ether 4′-nitrobenzo-15-crown-5 across a water/1,2-dichloroethane interface showed that the crown ether did not cross the interface but the complex formed by the crown ether with Na⁺ did transfer, the peak transfer current increased with increasing [Na⁺] until all the crown ether was complexed. The in situ interfacial second harmonic generation experiment indicates that, in the absence of Na⁺, the crown ether is oriented and ordered by the electric field at the interface. The sodium coronate shows a more complex behaviour at the interface.

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Investigation of transport across an immiscible liquid/liquid interface. Electrochemical and second harmonic generation studies

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