Probing the onset of crystallization of a microporous catalyst by combined X-ray absorption spectroscopy and X-ray diffraction

Gopinathan Sankar; John Meurig Thomas; Fernando Rey; G. Neville Greaves

doi:10.1039/C39950002549

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Journal of the Chemical Society, Chemical Communications

Issue 24, 1995

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Probing the onset of crystallization of a microporous catalyst by combined X-ray absorption spectroscopy and X-ray diffraction

Gopinathan Sankar , John Meurig Thomas , Fernando Rey and G. Neville Greaves

J. Chem. Soc., Chem. Commun., 1995, 2549-2550

DOI: 10.1039/C39950002549

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Abstract
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The power of a new variant of the in situ combined XRA-XRD experiment (see ref. 12) is illustrated by tracking the inner shell environment and bonding of a Co^IIion as it changes, in the gel just prior to crystallisation, from octahedral to tetrahedral coordination, the state in which it finally appears in the microporcus catalyst CoAlPO-5: the technique is widely applicable.

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Journal of the Chemical Society, Chemical Communications

Probing the onset of crystallization of a microporous catalyst by combined X-ray absorption spectroscopy and X-ray diffraction

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