Cyclophanes with self-recognising components

Pier-Lucio Anelli; Masumi Asakawa; Peter R. Ashton; George R. Brown; Wayne Hayes; Oldrich Kocian; Santiago Rodríguez Pastor; J. Fraser Stoddart; Malcolm S. Tolley; Andrew J. P. White; David J. Williams

doi:10.1039/C39950002541

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Journal of the Chemical Society, Chemical Communications

Issue 24, 1995

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Cyclophanes with self-recognising components

Pier-Lucio Anelli , Masumi Asakawa , Peter R. Ashton , George R. Brown , Wayne Hayes , Oldrich Kocian , Santiago Rodríguez Pastor , J. Fraser Stoddart , Malcolm S. Tolley , Andrew J. P. White and David J. Williams

J. Chem. Soc., Chem. Commun., 1995, 2541-2545

DOI: 10.1039/C39950002541

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Abstract
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High dilution techniques have been employed to construct a series of charged flexible cyclophanes comprised of π-electron-rich hydroquinone and π-electron-deficient bipyridinium residues linked by polyether spacer units of varying length: significant conformational changes, leading to intramolecular and intermolecular interactions between the π-donors and π-acceptors, have been observed—as evidenced by X-ray crystallographic and variable temperature ¹H NMR and 2D ROESY spectroscopic investigations—within the series of the cyclophanes both in the solid and solution states as a result of increasing the lengths of the polyether spacer units.

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Journal of the Chemical Society, Chemical Communications

Cyclophanes with self-recognising components

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