Total synthesis of milbemycin G: assembly and completion of the synthesis

Simon Bailey; Aphiwat Teerawutgulrag; Eric J. Thomas

doi:10.1039/C39950002521

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Journal of the Chemical Society, Chemical Communications

Issue 24, 1995

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Total synthesis of milbemycin G: assembly and completion of the synthesis

Simon Bailey , Aphiwat Teerawutgulrag and Eric J. Thomas

J. Chem. Soc., Chem. Commun., 1995, 2521-2522

DOI: 10.1039/C39950002521

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Abstract
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The Wittig reaction between phosphonium salt 1 and the hydroxybutenolide 2 followed by deprotection, macrocyclisation, and reduction gives the 6-hydroxymilbemycin E 9 which by further cyclisation is converted into milbemycin G 11.

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Journal of the Chemical Society, Chemical Communications

Total synthesis of milbemycin G: assembly and completion of the synthesis

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