Easy access to C,C′-bifunctionalized 1H-phosphirene–tungsten complexes: evidence for ambiphilic reaction behaviour of a phosphanediyl–tungsten complex

Annette Ostrowski; Jörg Jeske; Peter G. Jones; Rainer Streubel

doi:10.1039/C39950002507

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Journal of the Chemical Society, Chemical Communications

Issue 24, 1995

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Easy access to C,C′-bifunctionalized 1H-phosphirene–tungsten complexes: evidence for ambiphilic reaction behaviour of a phosphanediyl–tungsten complex

Annette Ostrowski , Jörg Jeske , Peter G. Jones and Rainer Streubel

J. Chem. Soc., Chem. Commun., 1995, 2507-2508

DOI: 10.1039/C39950002507

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Abstract
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The 2H-azaphosphirene–tungsten complex 1 reacts with ethoxyacetylene 2a or dimethyl acetylenedicarboxylate 2b to yield C,C′-bifunctionalized 1H-phosphirene–tungsten complexes 4a,b; compounds 4a,b are characterized by NMR spectroscopy (¹³C, ³¹P) and complex 4a by single-crystal X-ray diffraction.

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Easy access to C,C′-bifunctionalized 1H-phosphirene–tungsten complexes: evidence for ambiphilic reaction behaviour of a phosphanediyl–tungsten complex

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