Highly selective monotetrahydropyranylation of symmetrical diols catalysed by a strongly acidic ion-exchange resin

Takeshi Nishiguchi; Masahumi Kuroda; Masahiko Saitoh; Akiko Nishida; Shizuo Fujisaki

doi:10.1039/C39950002491

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Journal of the Chemical Society, Chemical Communications

Issue 24, 1995

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Highly selective monotetrahydropyranylation of symmetrical diols catalysed by a strongly acidic ion-exchange resin

Takeshi Nishiguchi , Masahumi Kuroda , Masahiko Saitoh , Akiko Nishida and Shizuo Fujisaki

J. Chem. Soc., Chem. Commun., 1995, 2491-2492

DOI: 10.1039/C39950002491

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Abstract
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Several primary and secondary symmetrical diols, ranging from propane-1,3-diol to decane-1,10-diol, are selectively monoprotected by monotetrahydropyranyl ether formation catalysed by a strongly acidic ion-exchange resin (Dowex 50w × 2, 50–100 mesh) in a 3,4-dihydro-2H-pyran-hydrocarbon mixture.

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Takeshi Nishiguchi
Masahumi Kuroda
Masahiko Saitoh
Akiko Nishida
Shizuo Fujisaki

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Journal of the Chemical Society, Chemical Communications

Highly selective monotetrahydropyranylation of symmetrical diols catalysed by a strongly acidic ion-exchange resin

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