Novel insertion of dimethylsilanone into an Yb–N bond and molecular structure of the insertion product [{Yb(η2-C3N2HMe2-3,5)(µ-η1:η2-OSiMe2C3N2HMe2-3,5)(η-C5H4Me)}2]

Xigeng Zhou; Huaizhu Ma; Xiaoying Huang; Xiaozeng You

doi:10.1039/C39950002483

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Journal of the Chemical Society, Chemical Communications

Issue 24, 1995

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Novel insertion of dimethylsilanone into an Yb–N bond and molecular structure of the insertion product [{Yb(η₂-C₃N₂HMe₂-3,5)(µ-η¹:η²-OSiMe₂C₃N₂HMe₂-3,5)(η-C₅H₄Me)}₂]

Xigeng Zhou , Huaizhu Ma , Xiaoying Huang and Xiaozeng You

J. Chem. Soc., Chem. Commun., 1995, 2483-2484

DOI: 10.1039/C39950002483

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When [Yb(C₃N₂HMe₂-3,5)(C₅H₄Me)](C₃N₂H₂Me₂-3,5 = 3,5-dimethylpyrazole) is recrystallized by slow diffusion of hexane into a thf solution which contains a small amount of dimethylsilicone grease, it is converted into to the unexpected complex [{Yb(η₂-C₃N₂HMe₂-3,5)(µ-η¹:η²-OSiMe₂C₃N₂HMe₂-3,5)(η-C₅H₄Me)}₂] indicating a novel Me₂SiO insertion reaction.

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Journal of the Chemical Society, Chemical Communications

Novel insertion of dimethylsilanone into an Yb–N bond and molecular structure of the insertion product [{Yb(η₂-C₃N₂HMe₂-3,5)(µ-η¹:η²-OSiMe₂C₃N₂HMe₂-3,5)(η-C₅H₄Me)}₂]

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