Phosphine-mediated [2 + 2] cycloaddition of internal alk-2-ynoate and alk-2-ynone to [60]fullerene

Kou-Fu Liou; Chien-Hong Cheng

doi:10.1039/C39950002473

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Journal of the Chemical Society, Chemical Communications

Issue 24, 1995

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Phosphine-mediated [2 + 2] cycloaddition of internal alk-2-ynoate and alk-2-ynone to [60]fullerene

Kou-Fu Liou and Chien-Hong Cheng

J. Chem. Soc., Chem. Commun., 1995, 2473-2474

DOI: 10.1039/C39950002473

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Abstract
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Treatment of RCH₂C [triple bond, length half m-dash] CCOX with [60]fullerene in the presence of tricyclohexylphosphine (PCy₃) afforded a [2 + 2] cycloaddition product (1: R = H, X = OMe); 2: R = Bu, X = OMe; 3: R = X = Me which resulted from addition of the β, γ-carbons of RCH₂CCCOX to the carbon-carbon double bond across a 6/6 ring junction of [60]fullerene.

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Journal of the Chemical Society, Chemical Communications

Phosphine-mediated [2 + 2] cycloaddition of internal alk-2-ynoate and alk-2-ynone to [60]fullerene

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