Formation of novel photoadducts from irradiation of 5(S)-5-O-tert-butyldimethylsiloxymethylfuran-2(5H)-one

David Brown; Christine J. Cardin; John Mann

doi:10.1039/C39950000825

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Journal of the Chemical Society, Chemical Communications

Issue 8, 1995

Journal of the Chemical Society, Chemical Communications was published between 1972 - 1995.

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Formation of novel photoadducts from irradiation of 5(S)-5-O-tert-butyldimethylsiloxymethylfuran-2(5H)-one

David Brown, Christine J. Cardin and John Mann

J. Chem. Soc., Chem. Commun., 1995, 825-826

DOI: 10.1039/C39950000825

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Irradiation of 5S-5-O-tert-butyldimethylsiloxymethylfuran-2(5H)-one 1 in acetonitrile yields the C2-symmetric bis(lactone), 1S,2S,6S,7S-[3S,10S]-bis-tert-butyldimethylsiloxymethyl-4,9-dioxatricyclo[5.3.0.0^2,6]deca-5,8-dione 6, and a 3-substituted intramolecular product resulting from an apparent 8-endo-trig cyclisation.

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Formation of novel photoadducts from irradiation of 5(S)-5-O-tert-butyldimethylsiloxymethylfuran-2(5H)-one

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Journal of the Chemical Society, Chemical Communications

Formation of novel photoadducts from irradiation of 5(S)-5-O-tert-butyldimethylsiloxymethylfuran-2(5H)-one

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